Thermal oxidation activation of hydrochar for tetracycline adsorption: the role of oxygen concentration and temperature.
Identifieur interne : 000054 ( Main/Exploration ); précédent : 000053; suivant : 000055Thermal oxidation activation of hydrochar for tetracycline adsorption: the role of oxygen concentration and temperature.
Auteurs : Hua Huang [République populaire de Chine] ; Zhirui Niu [République populaire de Chine] ; Ruru Shi [République populaire de Chine] ; Jingchun Tang [République populaire de Chine] ; Lei Lv [République populaire de Chine] ; Jian Wang [République populaire de Chine] ; Yimo Fan [République populaire de Chine]Source :
- Bioresource technology [ 1873-2976 ] ; 2020.
Abstract
Poplar hydrochar (RHC) was activated by thermal oxidation (TA-O) in air at 300 °C (O300) and in air + N2 (0.5% O2) at 500 and 700 °C (O500 and O700), respectively, and in N2 at 300-700 °C (N300-N700) as control. Samples characterized by various methods were used to analyze their effect on tetracycline adsorption. The results showed that TA-O greatly increased adsorption capacity qe, 100 (mg·g-1, C0 = 100 mg·L-1) from 6.29 for RHC to 33.32, 96.23 and 60.90 for O300, O500 and O700, respectively. The O300 increased carboxyl and aromaticity whereas little influenced on porosity. The O500, with the highest SBET and Smicro, enhanced adsorption probably by micropore filling and π-π interactions. The O700 fused micropore into mesopore but decreased the SBET, Smicro and qe, 100. Thus, thermal oxidation at 500 °C and 0.5% O2 is recommended for hydrochar activation to absorb tetracycline.
DOI: 10.1016/j.biortech.2020.123096
PubMed: 32172087
Affiliations:
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Key Laboratory of Pollution Processes and Environmental Criteria (Ministry of Education), Tianjin Engineering Center of Environmental Diagnosis and Contamination Remediation, College of Environmental Science and Engineering, Nankai University, Tianjin 300071, China; Yan'an Key Laboratory of Environmental Monitoring and Remediation, Yan'an 716000, Shaanxi, China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>School of Petroleum Engineering and Environmental Engineering, Yan'an University, Yan'an 716000, Shaanxi, China; Key Laboratory of Pollution Processes and Environmental Criteria (Ministry of Education), Tianjin Engineering Center of Environmental Diagnosis and Contamination Remediation, College of Environmental Science and Engineering, Nankai University, Tianjin 300071, China; Yan'an Key Laboratory of Environmental Monitoring and Remediation, Yan'an 716000, Shaanxi</wicri:regionArea><wicri:noRegion>Shaanxi</wicri:noRegion></affiliation></author><author><name sortKey="Niu, Zhirui" sort="Niu, Zhirui" uniqKey="Niu Z" first="Zhirui" last="Niu">Zhirui Niu</name><affiliation wicri:level="1"><nlm:affiliation>School of Petroleum Engineering and Environmental Engineering, Yan'an University, Yan'an 716000, Shaanxi, China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>School of Petroleum Engineering and Environmental Engineering, Yan'an University, Yan'an 716000, Shaanxi</wicri:regionArea><wicri:noRegion>Shaanxi</wicri:noRegion></affiliation></author><author><name sortKey="Shi, Ruru" sort="Shi, Ruru" uniqKey="Shi R" first="Ruru" last="Shi">Ruru Shi</name><affiliation wicri:level="1"><nlm:affiliation>School of Petroleum Engineering and Environmental Engineering, Yan'an University, Yan'an 716000, Shaanxi, China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>School of Petroleum Engineering and Environmental Engineering, Yan'an University, Yan'an 716000, Shaanxi</wicri:regionArea><wicri:noRegion>Shaanxi</wicri:noRegion></affiliation></author><author><name sortKey="Tang, Jingchun" sort="Tang, Jingchun" uniqKey="Tang J" first="Jingchun" last="Tang">Jingchun Tang</name><affiliation wicri:level="1"><nlm:affiliation>Key Laboratory of Pollution Processes and Environmental Criteria (Ministry of Education), Tianjin Engineering Center of Environmental Diagnosis and Contamination Remediation, College of Environmental Science and Engineering, Nankai University, Tianjin 300071, China. Electronic address: tangjch@nankai.edu.cn.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>Key Laboratory of Pollution Processes and Environmental Criteria (Ministry of Education), Tianjin Engineering Center of Environmental Diagnosis and Contamination Remediation, College of Environmental Science and Engineering, Nankai University, Tianjin 300071</wicri:regionArea><placeName><settlement type="city">Tianjin</settlement></placeName></affiliation></author><author><name sortKey="Lv, Lei" sort="Lv, Lei" uniqKey="Lv L" first="Lei" last="Lv">Lei Lv</name><affiliation wicri:level="1"><nlm:affiliation>School of Petroleum Engineering and Environmental Engineering, Yan'an University, Yan'an 716000, Shaanxi, China; Yan'an Key Laboratory of Environmental Monitoring and Remediation, Yan'an 716000, Shaanxi, China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>School of Petroleum Engineering and Environmental Engineering, Yan'an University, Yan'an 716000, Shaanxi, China; Yan'an Key Laboratory of Environmental Monitoring and Remediation, Yan'an 716000, Shaanxi</wicri:regionArea><wicri:noRegion>Shaanxi</wicri:noRegion></affiliation></author><author><name sortKey="Wang, Jian" sort="Wang, Jian" uniqKey="Wang J" first="Jian" last="Wang">Jian Wang</name><affiliation wicri:level="1"><nlm:affiliation>School of Petroleum Engineering and Environmental Engineering, Yan'an University, Yan'an 716000, Shaanxi, China; Yan'an Key Laboratory of Environmental Monitoring and Remediation, Yan'an 716000, Shaanxi, China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>School of Petroleum Engineering and Environmental Engineering, Yan'an University, Yan'an 716000, Shaanxi, China; Yan'an Key Laboratory of Environmental Monitoring and Remediation, Yan'an 716000, Shaanxi</wicri:regionArea><wicri:noRegion>Shaanxi</wicri:noRegion></affiliation></author><author><name sortKey="Fan, Yimo" sort="Fan, Yimo" uniqKey="Fan Y" first="Yimo" last="Fan">Yimo Fan</name><affiliation wicri:level="1"><nlm:affiliation>School of Petroleum Engineering and Environmental Engineering, Yan'an University, Yan'an 716000, Shaanxi, China.</nlm:affiliation><country xml:lang="fr">République populaire de Chine</country><wicri:regionArea>School of Petroleum Engineering and Environmental Engineering, Yan'an University, Yan'an 716000, Shaanxi</wicri:regionArea><wicri:noRegion>Shaanxi</wicri:noRegion></affiliation></author></analytic><series><title level="j">Bioresource technology</title><idno type="eISSN">1873-2976</idno><imprint><date when="2020" type="published">2020</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Poplar hydrochar (RHC) was activated by thermal oxidation (TA-O) in air at 300 °C (O300) and in air + N<sub>2</sub> (0.5% O<sub>2</sub>) at 500 and 700 °C (O500 and O700), respectively, and in N<sub>2</sub> at 300-700 °C (N300-N700) as control. Samples characterized by various methods were used to analyze their effect on tetracycline adsorption. The results showed that TA-O greatly increased adsorption capacity q<sub>e, 100</sub> (mg·g<sup>-1</sup>, C<sub>0</sub> = 100 mg·L<sup>-1</sup>) from 6.29 for RHC to 33.32, 96.23 and 60.90 for O300, O500 and O700, respectively. The O300 increased carboxyl and aromaticity whereas little influenced on porosity. The O500, with the highest S<sub>BET</sub> and S<sub>micro</sub>, enhanced adsorption probably by micropore filling and π-π interactions. The O700 fused micropore into mesopore but decreased the S<sub>BET</sub>, S<sub>micro</sub> and q<sub>e, 100</sub>. Thus, thermal oxidation at 500 °C and 0.5% O<sub>2</sub> is recommended for hydrochar activation to absorb tetracycline.</div></front></TEI><pubmed><MedlineCitation Status="Publisher" Owner="NLM"><PMID Version="1">32172087</PMID><DateRevised><Year>2020</Year><Month>04</Month><Day>24</Day></DateRevised><Article PubModel="Print-Electronic"><Journal><ISSN IssnType="Electronic">1873-2976</ISSN><JournalIssue CitedMedium="Internet"><Volume>306</Volume><PubDate><Year>2020</Year><Month>Mar</Month><Day>03</Day></PubDate></JournalIssue><Title>Bioresource technology</Title><ISOAbbreviation>Bioresour Technol</ISOAbbreviation></Journal><ArticleTitle>Thermal oxidation activation of hydrochar for tetracycline adsorption: the role of oxygen concentration and temperature.</ArticleTitle><Pagination><MedlinePgn>123096</MedlinePgn></Pagination><ELocationID EIdType="pii" ValidYN="Y">S0960-8524(20)30365-5</ELocationID><ELocationID EIdType="doi" ValidYN="Y">10.1016/j.biortech.2020.123096</ELocationID><Abstract><AbstractText>Poplar hydrochar (RHC) was activated by thermal oxidation (TA-O) in air at 300 °C (O300) and in air + N<sub>2</sub> (0.5% O<sub>2</sub>) at 500 and 700 °C (O500 and O700), respectively, and in N<sub>2</sub> at 300-700 °C (N300-N700) as control. Samples characterized by various methods were used to analyze their effect on tetracycline adsorption. The results showed that TA-O greatly increased adsorption capacity q<sub>e, 100</sub> (mg·g<sup>-1</sup>, C<sub>0</sub> = 100 mg·L<sup>-1</sup>) from 6.29 for RHC to 33.32, 96.23 and 60.90 for O300, O500 and O700, respectively. The O300 increased carboxyl and aromaticity whereas little influenced on porosity. The O500, with the highest S<sub>BET</sub> and S<sub>micro</sub>, enhanced adsorption probably by micropore filling and π-π interactions. The O700 fused micropore into mesopore but decreased the S<sub>BET</sub>, S<sub>micro</sub> and q<sub>e, 100</sub>. Thus, thermal oxidation at 500 °C and 0.5% O<sub>2</sub> is recommended for hydrochar activation to absorb tetracycline.</AbstractText><CopyrightInformation>Copyright © 2020 Elsevier Ltd. All rights reserved.</CopyrightInformation></Abstract><AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>Huang</LastName><ForeName>Hua</ForeName><Initials>H</Initials><AffiliationInfo><Affiliation>School of Petroleum Engineering and Environmental Engineering, Yan'an University, Yan'an 716000, Shaanxi, China; Key Laboratory of Pollution Processes and Environmental Criteria (Ministry of Education), Tianjin Engineering Center of Environmental Diagnosis and Contamination Remediation, College of Environmental Science and Engineering, Nankai University, Tianjin 300071, China; Yan'an Key Laboratory of Environmental Monitoring and Remediation, Yan'an 716000, Shaanxi, China.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Niu</LastName><ForeName>Zhirui</ForeName><Initials>Z</Initials><AffiliationInfo><Affiliation>School of Petroleum Engineering and Environmental Engineering, Yan'an University, Yan'an 716000, Shaanxi, China.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Shi</LastName><ForeName>Ruru</ForeName><Initials>R</Initials><AffiliationInfo><Affiliation>School of Petroleum Engineering and Environmental Engineering, Yan'an University, Yan'an 716000, Shaanxi, China.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Tang</LastName><ForeName>Jingchun</ForeName><Initials>J</Initials><AffiliationInfo><Affiliation>Key Laboratory of Pollution Processes and Environmental Criteria (Ministry of Education), Tianjin Engineering Center of Environmental Diagnosis and Contamination Remediation, College of Environmental Science and Engineering, Nankai University, Tianjin 300071, China. Electronic address: tangjch@nankai.edu.cn.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Lv</LastName><ForeName>Lei</ForeName><Initials>L</Initials><AffiliationInfo><Affiliation>School of Petroleum Engineering and Environmental Engineering, Yan'an University, Yan'an 716000, Shaanxi, China; Yan'an Key Laboratory of Environmental Monitoring and Remediation, Yan'an 716000, Shaanxi, China.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Wang</LastName><ForeName>Jian</ForeName><Initials>J</Initials><AffiliationInfo><Affiliation>School of Petroleum Engineering and Environmental Engineering, Yan'an University, Yan'an 716000, Shaanxi, China; Yan'an Key Laboratory of Environmental Monitoring and Remediation, Yan'an 716000, Shaanxi, China.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Fan</LastName><ForeName>Yimo</ForeName><Initials>Y</Initials><AffiliationInfo><Affiliation>School of Petroleum Engineering and Environmental Engineering, Yan'an University, Yan'an 716000, Shaanxi, China.</Affiliation></AffiliationInfo></Author></AuthorList><Language>eng</Language><PublicationTypeList><PublicationType UI="D016428">Journal Article</PublicationType></PublicationTypeList><ArticleDate DateType="Electronic"><Year>2020</Year><Month>03</Month><Day>03</Day></ArticleDate></Article><MedlineJournalInfo><Country>England</Country><MedlineTA>Bioresour Technol</MedlineTA><NlmUniqueID>9889523</NlmUniqueID><ISSNLinking>0960-8524</ISSNLinking></MedlineJournalInfo><CitationSubset>IM</CitationSubset><KeywordList Owner="NOTNLM"><Keyword MajorTopicYN="N">Hydrochar</Keyword><Keyword MajorTopicYN="N">Oxygen concentration</Keyword><Keyword MajorTopicYN="N">Temperature</Keyword><Keyword MajorTopicYN="N">Tetracycline</Keyword><Keyword MajorTopicYN="N">Thermal activation</Keyword></KeywordList><CoiStatement>Declaration of Competing Interest The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper.</CoiStatement></MedlineCitation><PubmedData><History><PubMedPubDate PubStatus="received"><Year>2019</Year><Month>12</Month><Day>19</Day></PubMedPubDate><PubMedPubDate PubStatus="revised"><Year>2020</Year><Month>02</Month><Day>27</Day></PubMedPubDate><PubMedPubDate PubStatus="accepted"><Year>2020</Year><Month>02</Month><Day>28</Day></PubMedPubDate><PubMedPubDate PubStatus="pubmed"><Year>2020</Year><Month>3</Month><Day>17</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="medline"><Year>2020</Year><Month>3</Month><Day>17</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="entrez"><Year>2020</Year><Month>3</Month><Day>16</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate></History><PublicationStatus>aheadofprint</PublicationStatus><ArticleIdList><ArticleId IdType="pubmed">32172087</ArticleId><ArticleId IdType="pii">S0960-8524(20)30365-5</ArticleId><ArticleId IdType="doi">10.1016/j.biortech.2020.123096</ArticleId></ArticleIdList></PubmedData></pubmed><affiliations><list><country><li>République populaire de Chine</li></country><settlement><li>Tianjin</li></settlement></list><tree><country name="République populaire de Chine"><noRegion><name sortKey="Huang, Hua" sort="Huang, Hua" uniqKey="Huang H" first="Hua" last="Huang">Hua Huang</name></noRegion><name sortKey="Fan, Yimo" sort="Fan, Yimo" uniqKey="Fan Y" first="Yimo" last="Fan">Yimo Fan</name><name sortKey="Lv, Lei" sort="Lv, Lei" uniqKey="Lv L" first="Lei" last="Lv">Lei Lv</name><name sortKey="Niu, Zhirui" sort="Niu, Zhirui" uniqKey="Niu Z" first="Zhirui" last="Niu">Zhirui Niu</name><name sortKey="Shi, Ruru" sort="Shi, Ruru" uniqKey="Shi R" first="Ruru" last="Shi">Ruru Shi</name><name sortKey="Tang, Jingchun" sort="Tang, Jingchun" uniqKey="Tang J" first="Jingchun" last="Tang">Jingchun Tang</name><name sortKey="Wang, Jian" sort="Wang, Jian" uniqKey="Wang J" first="Jian" last="Wang">Jian Wang</name></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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